Skip to main content
Industrial Research And Consultancy Centre
Patent
Method for gelation temperature measurement of waxy crude oil without disturbing crystal network
Problem Statement

Ensuring consistent flow in waxy crude oil pipelines is difficult due to the gelation of waxy crude oil under low-temperature conditions, requiring higher pressures to restart flow in gelled pipelines.

Abstract

Flow assurance in waxy crude oil pipelines is challenging due to gelation at low temperatures. This study introduces a novel method for measuring gelation temperature using the evolution of normal force in a rheometer geometry. This new Non-oscillatory non-rotary (NONR) method provides accurate and repeatable results without the need for gel movement. The results align well with existing methods, making it a reliable alternative.

Uniqueness of the Solution
  • Measures gelation temperature using the evolution of normal force as a function of temperature in a rheometer 
  • Avoids the influence of shear stress or shear rate, providing more precise measurements 
  • Demonstrates good repeatability and accuracy for both model waxy oil and real crude oils 
  • Effective under static conditions without requiring gel movement 
  • Applicable to other materials exhibiting thermal shrinkage during cooling
Current Status of Technology

The Non-oscillatory non-rotary (NONR) method has been validated through experiments and comparison with existing methods, showing good agreement and repeatability. A prototype is currently being developed.

Technology readiness level

9

Societal Impact

Improving the accuracy of gelation temperature measurements can enhance the reliability and efficiency of crude oil transportation, reducing the risk of pipeline blockages and associated environmental hazards.

Relevant Industries, Domains and Applications

Oil and gas exploration and production, Pipeline transportation, Rheological research

Applications or Domain
  • Oil and gas industry, particularly in flow assurance for subsea pipelines 
  • Research and development in rheology and materials science

Geography of IP

Type of IP

Application Number

202121022815

Filing Date
Grant Number

423309

Grant Date
Assignee(s)
Indian Institute of Technology Bombay
**This IP is owned by IIT Bombay**