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Industrial Research And Consultancy Centre
Patent
A Process for Preparing Polymer Nanocomposites Nanocubons
Abstract

The present invention relates to polymer nanocomposites comprising nanocubons with uniform size and morphology, along with a process for their preparation. These nanocubons exhibit desirable dielectric properties, making them suitable as nanofillers for electrical insulation in electronic devices. Unlike conventional ceramic fillers, these nanocubons avoid drawbacks such as bulkiness, increased viscosity, and conductivity risks, thus offering enhanced compatibility and performance in applications requiring thermal regulation and dielectric strength.

Figure 1. PPC NPs was optimized in THF organic solvent electron microscopy. (Image a: represents shape and size, Image b: represents population distribution, Image c-i: represents semi-crystalline surface morphology, and Image c-ii: represents amorphous diffraction pattern).

Problem Statement

Conventional ceramic nanofillers used in electronic and fluid systems enhance dielectric and thermal properties but face key drawbacks—bulkiness, poor dispersion, increased viscosity, and unintended electrical conductivity. There is a need for alternative nanofillers that offer high dielectric strength and insulation without these limitations, especially for applications like sensors, medical devices, and pulse conditioning systems.

Uniqueness of the Solution
  • Dielectric Properties with Electrical Insulation: The nanocubons demonstrated strong dielectric behavior while maintaining electrical insulation due to the PPC (Poly (propylene carbonate)) matrix, overcoming the limitations of conventional ceramic fillers like high bulkiness, increased viscosity, and tunneling conductivity risks. 
  • No Aggregation or Settling: It has optimized particle size (100-250 nm) and uniform surface charge (zeta potential) that ensure long-term dispersion stability, solving problems such as nanoparticle settling or aggregation in nanofluids and composites. 
  • Semi-Crystalline Structure: The analysis revealed semi-crystalline morphology, offering a balance between strength and flexibility—ideal for medical, electronic and fluid insulation applications with strong dielectric behavior. 
  • Cost-Effective & Scalable Manufacturing: The Tetrahydrofuran (THF) synthesis process is simple, economical, and suitable for large-scale industrial production.
Prototype Details

The process for preparing nanocubons involves dissolving polypropylene carbonate (PPC) in tetrahydrofuran (THF) to form a solution, which is then emulsified with polyvinyl alcohol (1–5% w/v) to create a stable emulsion. This emulsion undergoes sonication (40% amplitude, 5s on/2s off pulses for 10 minutes) to ensure uniform particle distribution. The solvent is then evaporated, and nanocubons are isolated via centrifugation. The resulting nanocubons typically range in size from 100 to 250 nm.

Current Status of Technology

Currently at TRL 3 – proof of concept stage, with further development underway.

Technology readiness level

3

Societal Impact

The development of PPC-based Nanocubons nanofillers can significantly enhance the performance and miniaturization of electronic, biomedical, and energy storage devices.

Applications or Domain
  • Electronics 
  • Biomedical devices 
  • Sensor technology 
  • Nanotechnology 
  • Packaging industry 
  • Oil & Fluid technology

Geography of IP

Type of IP

Application Number

202121007979

Filing Date
Grant Number

434460

Grant Date
Assignee(s)
Indian Institute of Technology Bombay
**This IP is owned by IIT Bombay**